SLCO SQUID
Experimental investigation on the order parameter symmetry of the superconducting
Sr1 xLaxCuO2 thin films using SQUIDs

Project code: PN-II-ID-PCE-2011-3-1065, contract no. 179/07.10.2011

 

 

 

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Project results

 

I. Publications in ISI journals

     
    1. J. Tomaschko, S. Scharinger, V. Leca, J. Nagel, M. Kemmler, T. Selistrovski, S. Diebold, J. Jochum, R. Kleiner, and D. Koelle, Phase-sensitive evidence for dx2-y2 pairing symmetry in the parent-structure high-Tc cuprate superconductor Sr1-xLaxCuO2, Physical Review B 86, 094509 (2012) [download paper]

    1. J. Tomaschko, V. Leca, T. Selistrovski, S. Diebold, J. Jochum, R. Kleiner, and D. Koelle, Properties of the electron-doped infinite-layer superconductor Sr1-xLaxCuO2 epitaxially grown by pulsed laser deposition, Physical Review B 85, 024519 (2012) [download paper]

 

II. Conferences (oral presentations and posters)

  1. V. Leca, J. Tomaschko, M. Danila, D. Wang, W. A. Bik, R. Kleiner, and D. Koelle, Closing the circle: d-wave order parameter symmetry in the electron‑doped Sr1-xLaxCuO2 superconductors, COST TO-BE Spring Meeting 2015, Aveiro, Portugal, 30th March - 2nd April (2015), invited talk [download presentation]
  2. M. Danila, V. Leca, J. Tomaschko, D. Wang, W. M. Arnoldbik, R. Kleiner, and D. Koelle, Defects network and transport properties in electron-doped Sr1-xLaxCuO2 thin films grown by laser ablation, 28th International Conference on Defects in Semiconductors, July 27 – 31, Espoo, Finland (2015) [download poster]
  3. V. Leca, J. Tomaschko, M. Danila, D. Wang, W. A. Bik, R. Kleiner, and D. Koelle, Strain relaxation and superconductivity in electron-doped Sr1-xLaxCuO2 thin films grown by laser ablation, International Conference on Superconductivity and Magnetism-ICSM 2014, Istanbul, Turkey (2014) [download presentation]
  4. V. Leca, J. Tomaschko, M. Danila, Di Wang, W. A. Bik, D. Koelle, and R. Kleiner, Application of SQUIDs to phase-sensitive experiments, Electroceramics XIV conference, Bucharest, Romania (2014) [download presentation]
  5. V. Leca, J. Tomaschko, D. Wang, M. Danila, W. A. Bik, R. Kleiner si D. Koelle, Superconducting Sr0.85La0.15CuO2 bicrystal grain boundary Josephson junctions, 11th European Conference on Applied Superconductivity - EUCAS, Genova, Italia (2013) [download presentation]
  6. V Leca, J. Tomaschko, M. Danila, W. A. Bik, A. Oprisa, R. Kleiner si D. Koelle, Structural and electrical properties in superconducting Sr0.85La0.15CuO2-based nanostructures, International Conference on Superconductivity and Magnetism - ICSM, Istanbul, Turcia (2012) [download presentation]

 

III. Training periods abroad

 

2011:
1. University of Tübingen, Institute of Physics, Department of Experimental Physics II (Tübingen, Germany). Period: 5.11-10.12 2011
Scope: Pulsed laser deposition and characterization (XRD, AFM, R vs. T) of Sr1-xLaxCuO2 thin films grown on (001) SrTiO3 and (001) KTaO3 substrates.

2012:
1. University of Tübingen, Institute of Physics, Department of Experimental Physics II (Tübingen, Germany). Period: 20.05-07.06.2012
Scope: Development of the technology for fabrication of the Sr1-xLaxCuO2/Au/Nb ramp-type Josephson junctions. Preliminary studies.
2. Karlsruhe Institute of Technology (Karlsruhe, Germany). Period: 23 – 26.09.2012
Scope: High Resolution Transmission Electron Microscopy (HRTEM and EELS) on Sr1-xLaxCuO2 thin films and Sr1-xLaxCuO2/Au/Nb ramp-type Josephson junctions.
3. University of Tübingen, Institute of Physics, Department of Experimental Physics II (Tübingen, Germany). Period: 10-25.10.2012
Scope: Development of the technology for fabrication of the Sr1-xLaxCuO2-based SQUIDs. Preliminary studies.

2013:
1. University of Twente, Faculty of Science and Technology, Inorganic Materials Science Group (Enschede, The Netherlands). Period: 29.01 – 03.02.2013 Scope: Advanced Pulsed Lased Deposition of Complex Oxides course.
2. University of Tübingen, Institute of Physics, Department of Experimental Physics II (Tübingen, Germany). Period: 02-16.06.2013
Scope: Development of the technology for fabrication of the Sr1-xLaxCuO2-based grain boundary Josephson junctions. Preliminary studies.
Travel and hotel costs covered by the Department of Experimental Physics II, University of Tübingen.
3. University of Tübingen, Institute of Physics, Department of Experimental Physics II (Tübingen, Germany). Period: 25.08-07.09.2013
Scope: Low temperature electrical and magnetic measurements on grain boundary Sr1-xLaxCuO2-based SQUIDs.
Travel and hotel costs covered by the Department of Experimental Physics II, University of Tübingen
4. University of Tübingen, Institute of Physics, Department of Experimental Physics II (Tübingen, Germany). Period: 17-30.11.2013
Scope: Pulsed laser deposition and characterization (XRD, AFM, R vs. T) of Sr1-xLaxCuO2 thin films grown on (110) DyScO3 substrates.
Travel and hotel costs covered by the Department of Experimental Physics II, University of Tübingen

 

IV. Acquisition of new equipments

 

I. Tube oven with controlable atmosphere (O2, N2, Ar).


    Manufacturer: NABERTHERM (Germany)
    Model: R50

    Price: 4700 € (+ 24% VAT)
    Status: operational since 02.2013

    Characteristics:

    Compact tabletop tube furnaces with integrated control systems; equipped with a working tube of C 530 ceramic and two fiber plugs, Tmax of 1200C. Housing made of sheets of textured stainless steel, outer tube diameter of 50 mm, heated length tube of 450 mm, type S thermocouple, solid state relays for low noise operation. Program controller B 180, Digital PID-temperature control, one storable program, timer for delayed start, over-temperature protection, auto tune, integrated KW/hr counter, integrated operating hours counter.

    Gas supply systems for nitrogen and oxygen (one for each) with shutoff valve and flow meter with control valve (volume 50-500 l/hr), 2 plugs of ceramic fiber with protective connections. Oven dimensions: 400x240x490 mm3 (WxDxH), weight of 20 kg.

    The oven is installed at IMT-Bucharest.

       

    II. Ar-ion milling system

     

    Manufacturer: TSST (The Netherlands)
    Price: 65 k€ (+ 24% VAT)
    Status: operational since 12.2013

     

    The system uses Ar ions for physical etching (milling) of the material (metals, oxides, polymers) and angles from 0 to 90o (vs. the sample normal), with continuous sample rotation during etching.

    Characteristics:

    1. General characteristics

    - single chamber system containing an Ar-ion source for etching;

    - manual loading of the wafers into the process chamber;

    - sealed, with vacuum (base pressure <5´10-6 mbar) and ventilation;

    - sample rotation and tilt (0-90o) during etching;

    - process monitoring software;

    - it can be used as loadlock in case of a future upgrade (one free port);

    - safe shut down procedure.

     

    2. The process chamber
    The chamber is equipped with an Ar-ion milling unit that ensures high quality anisotropic etching of single crystal and amorphous materials with etching rates as low as 0.10 nm/s, with etching non-uniformity on a 1” wafer of less than 5% and non-uniformity from run to run less than 5%. The chamber is equipped with a sample holder that allows continuous rotation during Ar-ion milling, as well as manual tilting of the sample between 0 to 90o. The sample holder is equipped with cooling with Ar gas for cooling the sample during Ar-ion milling process. The chamber has an access door for loading/unloading the samples with an window for monitoring the sample during processes. The system is equipped with a free port for future connection of a magnetic manipulator for manual transfer of the samples between this chamber and another process chamber, without breaking the vacuum; equipped with the required gas line connections for Ar-ion milling and for flooding the chamber (N2). Pressure control (pressure gauge, mass flow controller, etc) and electronics (for Ar-ion milling, pressure control, etc).

     

    3. Operation
    The system is used for etching by Ar-ions of oxides, metals, polymers; it allows tilting of the sample at angles of 0-90o between the Ar-ion beam and the normal to the sample surface (manual control of the tilt angle), and with continuous rotation of the sample holder during etching. The sample-ion source distance can be modified within 10 cm. The sample transfer is done manually. Software control of the process.

     

    4. Main parameters of the system
    4.1. Ar-ion source
    Gridded ion source (4 cm diameter), with power supply for 220 V/50 Hz, and control electronics; beam voltage variable between 200-1200 V dc, beam current > 20 mA, for variable beam energy; the gas line for the source is equipped with a mass flow controller; the ion source is equipped with a neutralizer; the ion source permits changing the duration of the milling (ON/OFF sequences).

     

    4.2. Sample stage of the chamber
    The sample permits automatic sample rotation during Ar-ion milling process, manual tilting over 0-90o range, and is equipped with a manual Z-shifter that allows the Ar-ion source to substrate distance to be varied over 100 mm;

    The system is installed at IMT-Bucharest.

 


Contact info:

Dr. Victor Leca
Center of Nanotechnology, Laboratory for Molecular Nanotechnology
National Institute for Research and Development in Microtechnologies - IMT Bucharest
Address: 126A, Erou Iancu Nicolae Street R-077190, Voluntari, Ilfov, Romania
Tel: +40-21-269.07.70 (ext. 33)
Fax: +40-21-269.07.72
E-Mail: victor[dot]leca[at]imt[dot]ro
.